ISO-CHEK Cassettes
Suitable for most isocyanates, the patented‡ ISO-CHEK sampling system uses a two-stage filter that results in the simultaneous collection and separation of vapour from aerosol at the point of collection.
Description
- Accurately samples diisocyanates: HDI, MDI, IPDI, HMDI, 2,4-TDI, and 2,6-TDI
- The only filter-based system that simultaneously traps and separates both monomers and oligomers
- For better determinations of control strategies
- Decreases sample preparation and analysis time by 40% compared to other methods
- Pre-made calibration standards are available
- Highly stable — minimizes storage and handling
- Highly sensitive analysis provides detection limits below current regulated exposure levels
- Ideal for occupational sampling and environmental surveys
- Requires only a 15-minute sample time
- Meets the specifications of several methods
- ASTM D5932 for 2,4, 2,6-TDI
- ASTM D6561 for HDI
- ASTM D6562 for HDI
‡ U.S Patent No. 4,961,916
Specifications
| Collection Method | Dual filter cassette; 5-µm PTFE membrane traps aerosol phase, glass fibre filter impregnated with MAMA collects vapour phase |
| Sample Flow Rate | 1 L/min |
| Sample Time | 15 minutes |
| Derivatizing Reagent (filter coating for vapour phase) | 9-(N-methylaminomethyl) anthracene (MAMA) |
| Derivatizing Solution (for aerosol phase) | 1-(2-Methoxyphenyl) piperazine (MOPIP) |
| Supplied in jars containing 5 ml of solution (0.5 mg MOPIP in 5 ml toluene) | |
| Sample Stability | Can be stored at 4°C (39.2°F) for up to 10 days. Store and prepare in solvent-free environments. SKC recommends sample analysis as soon as possible. |
| Analysis | Reverse phase HPLC with UV and fluorescence detection (FD) |
| Quantitation Limit | 0.15 ppb for 2,4-TDI, 2,6-TDI, 1,6-HDI, IPDI, MDI, HMDI monomer |
| 1.5 ppb for 1,6-HDI and MDI oligomers | |
| Limit of Detection | 0.2 mg/m3 for 2,4-TDI and 2,6-TDI |
| 0.6 mg/m3 for 1,6-HDI | |
| 0.3 (UV)/0.08 (FD) mg/m3 for MDI † | |
| † First number is with UV detector, the second is with a fluorescence detector (FD) | |
ISO-CHEK Cassettes
| Description | Pack Size | Part Number |
| ISO-CHEK Sampling Cassettes *, preloaded clear cassettes for isocyanates, requires Derivatizing Solution | 12 | 225-9022 |
| 36 | 225-9022A | |
| * Limited shelf-life – see Specifications – Sample Stability | ||
Accessories
| Description | Pack Size | Part Number |
| Jars, 37 mm with PTFE-lined cap. Suitable for for transporting and solvent extraction of filter samples in the field or laboratory. | 36 | 225-8377 |
| Calibration Standard †, MAMA-HDI, 1 g | Each | 225-9053 |
| Calibration Standard †, MAMA-HMDI, 1 g | Each | 225-9056 |
| Calibration Standard †, MAMA-IPDI, 1 g | Each | 225-9054 |
| Calibration Standard †, MAMA-MDI, 1 g | Each | 225-9062 |
| Calibration Standard †, MAMA-2,4-TDI and 2,6-TDI, 1 g | Each | 225-9052 |
| Calibration Standard Set †, HDI, MDI, IPDI, 2,4-TDI, 2,6-TDI, 1 g each | Set | 225-9055 |
| Packaging Kit, materials for shipping 10 packages of samplers and jars | Each | 225-9059 |
| * Limited shelf-life | ||
| † Limited shelf-life, freezer storage recommended; refrigerated shipping not required. See Specifications – Sample Stability | ||
Documentation
